Focuses on basic aspects of nano/microfibers made by electrospinning, with details on spinning recipes, characterization techniques, and the chemistry of the polymers in use. The basic understanding provided in the book is useful for producing 1D and 3D fibrous structures with specific properties for applications such as textiles, membranes, reinforcements, catalysis, filters, or biomedical uses. Students and practitioners will find great value in the step-by-step instructions on how to manufacture nanofibers. Topics include electrospinning equipment, history of electrospinning and nanofibers, characterization, fundamentals of electrospun fibers, ready-made recipes for spinning solutions, conditions for the production of highly diverse fiber morphologies and arrangements, and the chemistry of fiber-forming materials.