"Synchrotron Techniques in Interfacial Electrochemistry" offers a comprehensive examination of the structure of the electrode-solution interface and surface films. The book addresses the theoretical foundations of X-ray scattering at surfaces and interfaces, as well as the instrumentation of synchrotron radiation. It highlights various techniques such as surface X-ray diffraction, X-ray reflectivity, and X-ray absorption spectroscopy (EXAFS and XANES). Additionally, standing wave techniques and infrared spectroscopy are discussed. The application of each technique to investigate electrochemical issues is clearly presented, making the book a valuable resource for professionals and students in the field of electrochemistry.